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Hexacarbonyl diiron complexes of N-substituted sulfimides (SNR) have been obtained from the parent tetrahedrane, Fe2(CO) 6 (μ-SNH) (1), by deprotonation to give the anion Fe 2 (CO) 6 (μ-SN - ) (2) and subsequent reaction with either trialkyloxonium or carbenium tetrafluoroborates. The new aza-diferra-thia-tetrahedranes, Fe 2 (CO) 6 (μ-SNR) (R = CH 3  (3a), C 2 H 5  (3b), CPh 3  (3c), cyclo-C 3 Ph 3  (3d), cyclo-C 7 H 7  (3e), and cyclo-(C 7 H 7 )M (CO) 3  with M = Cr (3f), Mo (3g), W (3h)) were characterized by their  1 H and  13 C NMR as well as their IR and MS spectra. The molecular structure of Fe 2 (CO) 6 [SN-cyclo-C 7 H 7 Mo(CO) 3 ] (3g) has been determined by X-ray diffraction.

Hexacarbonyldieisen-stabilisierte Sulfimid-Derivate, Fe 2 (CO) 6 (μ-SNR) / Hexacarbonyl Diiron Stabilized Sulfimide Derivatives, Fe 2 (CO) 6 (μ-SNR)