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Single crystals of the compounds MnFe(BO 3 )O (I) and MnAl 0.5 Y 0.5 (BO 3 )O (II), were obtained by a B 2 O 3  flux technique. I crystallizes with orthorhombic symmetry, space group D 16  2h  -Pnma (Nr.62), a = 939.92; b = 319.41; c = 939.11 pm; Z = 4 and II with monoclinic symmetry, space group C 5  2h -P2 1 /n (Nr. 14). a = 325.6; b = 955.1; c = 929.2 pm; β = 90.70° ; Z = 4. I is isotypic to the mineral Warwickite, while II is a distorded variant of this structure. All metal ions are octahedrally coordinated. Both structures contain isolated, trigonal planar BO 3  units and oxygen atoms that are not coordinated to boron.

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Zur Synthese und Kristallstruktur von manganhaltigen Boratoxiden: MnFe(BO 3 )O und MnAl 0,5 Y o,5 (BO 3 )O / Synthesis and Crystal Structure of Manganese Borate Oxides: MnFe(BO 3 )O and MnAl 0,5 Y o,5 (BO 3 )O