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Alkyl-1-thio-α/β-D-gaIactopyranosides (hexyl-dodecyl, 1a - g ) have been O-diethylborylated and then reduced with tetraethyldiboranes(6) in the presence of 9-methylsulfonyloxy- 9-borabicyclo[3.3.1]nonane (MSBBN) catalyst to give 1-alkylthio-1-deoxy-D-galactitols 3a -g after deprotection. 3 exhibit the smectic A liquid crystalline phase on melting.

Amphiphilic Carbohydrate-Based Mesogens, 11 Synthesis of Mesogenic 1-AIkylthio-1-deoxy-D-galactitols by Glycoside Reduction