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The heterocyclesEt [R 3  = Me: A; R 3  = C(Me)=CH 2 : B] react with 2-aminoethanethiol (1) by elimination of MeNH 2  to give the monocyclic[R = Me: 3a; R = C(Me)=CH 2 : 3b] and the thermically more stable bicyclic compounds[R = Me: 4a; R = C(Me)=CH 2 : 4b], 4a crystallizes in the monoclinic space group P2 1 /c [lattice constants (at 120 K) a = 9.3239(10), b = 8.9225(11), c = 17.3958(23) Å; β = 92.207(9)°] with a folded bicyclic ring system. cis-ClB(Et)C=C(Me)Si(Me 2 )Cl (C) and Na 2 -1BEt 3  (prepared from 1 and NaHBEt 3 ) form by elimination of MeNH 2  preferentially 3a and minor amounts of 4a. A reacts with o-aminothiophenol (2) via(5) to(6) and the products 7-10.

zeitschrift für naturforschung b

Organosubstituierte 1,6,2,5-Azoniathiasilaboratabicyclo[3.3.0]oct-3-ene - Herstellung und Kristallstruktur / Organosubstituted 1,6,2,5-A zoniathiasilaboratabicyclo[3.3.0]oct-3-enes - Preparation and Crystal Structure