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Li 2 P(2,4,6-Me 3 C 6 H 2 ) reacts with Cp°MoCl 2 (PMe 3 ) 2  (Cp° = C 5 Me 4 Et) with reductive cleavage of the Mo -Cp° bond to yield MoCl 2 (PMe 3 ) 2  (1). The reaction of the Mo(II) derivative MoCl 2 (PMe 3 ) 4  with two equivalents of KPPh 2 (dioxane) 2  yields [Mo(μ-PPh 2 )(PPh 2 )(PMe 3 )] 2  (2). Both have been characterized by X-ray crystal structure determination.

zeitschrift für naturforschung b

Synthese und Molekülstrukturen der Molybdän(II)-Komplexe MoCl 2 (PMe 3 ) 2  und [Mo(μ-PPh 2 )(PPh 2 )(PMe 3 )] 2  / Synthesis and Molecular Structures of the Molybdenum(II) Complexes MoCl 2 (PMe 3 ) 2  and [Mo(μ-PPh 2 )(PPh 2 )(PMe 3 )] 2