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Single crystals of Ag 0.5 Cu 3 V 0,5 Mo 2,5 O 12  have been prepared by crystallization from melts and investigated by X -ray methods. They crystallize with triclinic symmetry, space group C i  1  -P 1̄ , a = 6.797(6), b = 8.575(6), c = 9.897(7) Å, α = 103.47(6), β = 103.69(6), γ = 101.48(6)° and Z = 4. The crystal structure is characterized by chains of edge-sharing CuO 6  octahedra and CuO 5  pyramids. Special features of this com pound are the square planar surrounding of Ag +  by O 2−  and a statistical distribution of molybdenum and vanadium at one point position.

zeitschrift für naturforschung b

Ein Silber- Kupfer - Oxovanadato-Oxomolybdat mit Silber in quadratisch-planarer Koordination: Ag 0,5 Cu 3 V 0,5 Mo 2,5 O 12  / On a Silver Copper Oxovanadate-Oxomolybdate with Silver in Square Planar Coordination: Ag 0,5 Cu 3 V 0,5 Mo 2,5 O 12