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Single crystals of Hg 3 CrO 6  have been prepared by high pressure techniques (3600 bar oxygen, 600 °C). Hg 3 CrO 6  crystallizes with trigonal symmetry, space group D 6  3 —P3 2 12, a = 7.137(1), c = 10.017(2) Å, Z = 3. Nearly linear O—Hg—O dumb-bells are connected in planes, forming strongly puckered nets of six-membered rings. Each Hg 6 O 6  ring is centered by a CrO 4  tetrahedron; the CrO 4  tetrahedra are arranged in two equally occupied split positions.

zeitschrift für naturforschung b

Einkristallröntgenstrukturanalyse an Quecksilberchromat(VI): Hg 3 O 2 CrO 4  / Single Crystal X-Ray Structure Determination of a Mercury Chromate(VI): Hg 3 O 2 CrO 4