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Reactions of the organometallic phosphinimine Ph 3 P=N-SiMe 3  (1), with aqueous ReO 4  -  and  188 ReO 4  -  yield the ion pairs Ph 3 P=NH 2  + MO 4  -  (M=Re (2);  188 Re (4)). The ion pairs undergo dehydration upon heating to produce the neutral Re(VII) species: Ph 3 P=N-MO 3  (M=Re (3);  188 Re (5)). The solid state structure of Ph 3 P=NH 2  + ReO 4  -  (2) shows the presence of hydrogen bonding between the iminato hydrogen and the rhenium oxo center. The relevance of such reactions for the design of new radiopharmaceuticals is discussed

zeitschrift für naturforschung b

Organometallic Phosphinimines as Building Blocks for Potential New Radiopharmaceuticals. Synthesis, Structure and Reactivity of Ph 3 P=NH 2  + ReO 4  -