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Salts of the composition [M(N-MeIm) 6 ](SPh) 2  (M = Mn, Ni; N-MeIm = N-methylimidazole) were prepared by dissolution of the metal powders with N-MeIm solutions of Ph 2 S 2 . X-ray crystallographic examination established that these salts indeed feature uncoordinated PhS - . The salts [M(N-McIm) 6 ](SPh) 2  (M = Mn, Ni) react with S 8  to give [M(N-MeIm) 6 ]S 8  via the intermediacy of the perthiolate salts [M(N-MeIm) 6 ](S 2 Ph) 2 .

N-Methylimidazole Mediated Chemistry of Transition Metal Phenylthiolates. The Isolation of the Perthiolate Salts [M(N-MeIm) 6 ](S 2 Ph) 2