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The new π-donor bis-(phenylenedithio)-tetrathiafulvalene (5), synthesized via phosphite coupling of 2-oxo-1,3-dithiolo-[4,5b][1,4]-benzodithiin (4), has been prepared in 5 steps starting from 1,2-dimercaptobenzene and chloroacetyl chloride. Spectroscopic and electrochemical data point to a close similarity of 5 and dibenzo-tetrathiafulvalene (DB-TTF). 5 forms a highly conducting radical-cation salt (σ RT  = 100 S/cm) with AsF 6 - as counter ion.

Synthesis and Properties of Bis-(phenylenedithio)-tetrathiafulvalene (BPhDT-TTF): a New π-Donor for Organic Metals