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(PPh 4 ) 2 [Hg(Se 4 ) 2 ] has been prepared by the reaction of (PPh 4 ) 2 [Sn(Se 4 ) 3 ] with Hg(CH 3 COO) 2  in dimethylformamide (DMF) solution. [Cs(18-crown-6)] 2 [Hg 2 (Se 4 ) 3 ] has been prepared by the reaction of a lithium polyselenide solution in DMF with Hg(CH 3 COO) 2  in the presence of CsBr and 18-crown-6. Both compounds are obtained as dark red crystals and characterized by X-ray structure determinations.

zeitschrift für naturforschung b

Synthese und Kristallstrukturen der Polyselenido-Mercurate (PPh 4 ) 2 [Hg(Se 4 ) 2 ] und [Cs(18-Krone-6)] 2 [Hg 2 (Se 4 )3] / Syntheses and Crystal Structures of the Polyselenido Mercurates (PPh 4 ) 2 [Hg(Se 4 ) 2 ] and [Cs(18-Crown-6)] 2 [Hg 2 (Se 4 ) 3 ]