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Ruthenium thiolates [cpRu(PR′ 3 ) 2 (SR)] (PR′ 3  = PPh 3 ,1/2 dppe, 1/2 dppm, R = Me, CH 2 Ph) are obtained from the corresponding chlorides and NaSR. PPh 3  is readily exchanged for CO to give the chiral complexes [cpRu(PPh 3 )(CO)(SR)]. Alkylation with methyl tosylate yields the cations [cpRu(dppe)(SMeR)] +  and [cpRu(PPh 3 )(CO)(SMeR)] + , which were isolated as their PF 6  -  salts. The neutral carbonyls add dimethyl acetylenedicarboxylate giving five-membered metallocycles.

zeitschrift für naturforschung b

Elektronenreiche Ruthenium-Thiolat-Komplexe, Synthese und Reaktionen mit Elektrophilen / Electron-Rich Ruthenium Thiolate Complexes, Synthesis and Reactions with Electrophiles