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A novel cyclic nitrone spin trap 5,5-dimethyl-3-(2-ethoxycarbonylethyl)-1-pyrroline N-oxide has been prepared and its ability to trap a series of transient free radicals has been investigated. This nitrone scavenges free radicals to give persistent nitroxides, e.g., the half life-times of hydroxyl radical adducts and tert-butoxy radical adducts in benzene &amp;gt;30 min, and the life-time of acetyl adducts &amp;gt;60 min. The EPR spectrum of 2,2-dimethyl-4-(3-hydroxypropyl)pyrrolidinyl-1-oxyl aminoxyl shows that the hyperfine splitting constants of two

Synthesis and Plane Selective Spin Trapping of a Novel Trap 5,5-Dimethyl-3-(2-ethoxycarbonylethyl)-1-pyrroline N-oxide