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Potassium tungstate, K 2 WO 4 , decomposes at high pressures to give K 2 W 2 O 7  and other products. Single crystals of K 2 W 2 O 7  could be synthesized from a mixture of K 2 WO 4  + WO 3  at 40kbar, 1000 °C. The crystals are monoclinic, space group P2 1 /c, with a = 3.883(1) A, b = 13.653(4) Å, c = 5.960(1) Å, β = 90.40(3)°, and Ζ = 2.

zeitschrift für naturforschung b

Hochdrucksynthese und Kristallstruktur von Kalium- und Rubidiumdiwolframat(VI), K 2 W 2 O 7  und Rb 2 W 2 O 7  / High-Pressure Synthesis and Crystal Structure of Potassium and Rubidium Ditungstate(VI), K 2 W 2 O 7  und Rb 2 W 2 O 7