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The new ligand (Me 3 Si) 2  NC(Ph)NP(Ph) 2  N(SiMe 3 ) (1) reacts with MOOCl  4  to yield the green metallacycle 4. 4 was characterized by X-ray diffraction. Crystals of 4 are monoclinic, space group P2 1 /n with a = 1061.2(10). b = 1590.5(10), c = 1737.4(20) pm, β = 104.84(7)° and Z = 4. Mo is coordinated octahedrally by two nitrogens of the bifunctional ligand. by one oxygen and three chlorine atoms. The ligand undergoes cyclization, a bond being formed between N and one phenylic o-position.

zeitschrift für naturforschung b

Synthese und Struktur eines ungewöhnlichen Molybdän-Heterocyclus durch Substitution eines Phenylringes in ortho-Stellung/ Synthesis and Structure of an Unusual Molybdenum Heterocycle by Substitution of a Phenyl Ring in ortho-Position