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(TTM-TTF) + [Ni(mnt) 2 ] -  and (TTM-TTF) +  [Pt(mnt) 2 ] -  {TTM-TTF = Tetra(methylthio)tetra- thiafulvalene. mnt = maleonitriledithiolate} were obtained as products of the reactions of TTM-TTF with [Et 4 N][Ni(mnt) 2 ] and [Et 4 N][Pt(mnt) 2 ]. (TTM-TTF) +  [Ni(mnt) 2 ] -  is tridinic. P1, a = 7.650(2), b = 9.671(3). c = 9.846(4) Å. α = 103.47(3)°, β = 101.76(3)°, γ = 91.73(3)°, V = 691 3  Å. Z = 1, d c  = 1.75 g cm -3 . For the isomorphous (TTM-TTF) + [Pt(mnt) 2 ] -  a = 7.749(2). b = 9.684(4). c = 9.883(3) Å, α = 103.31(2)°,β = 102.54(2)°, γ = 91.43(3)°, V = 702 Å 3  Z= 1, d c  = 2.04 g cm -3 . The structures consist of mixed stacks of the organic radical cations and of bis(maleonitriledithiolato)metal(III) anions.

zeitschrift für naturforschung b

1:1-Salze des organischen Donors Tetra(methylthio)tetrathiafulvalen und Bis(maleonitriIdithiolato)-Komplexen: (TTM-TTF) + [Ni(mnt) 2 ] -  und (TTM-TTF)+[ Pt(mnt) 2 ] -  / 1:1 Salts of the Organic Donor Tetra(methylthio)tetrathiafulvalene and Bis(maleonitriledithiolate) Complexes: (TTM -TTF) + [Ni(mnt)2] -  and (TTM -TTF) + [Pt(mnt) 2 ] -