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Syntheses of oxovanadium(V) thiolates such as O = V(SR) 3  (R =  t C 4 H 9  , SiPh 3  ) and O=V(O t C 4 H 9  ) n (S t C 4 H 9 ) 3-n (n = 1, 2) are described. The thiovanadium(V) compounds S=V(O t C 4 H 9  ) 3  , S = V(S t C 4 H 9 )(O t C 4 H 9 ) 2 and S=V(SSiPh 3 ) 3  have been prepared by various methods :substitionusing Lawesson reagent, oxidation of V(O t C 4 H 9 ) 4  by sulfur, or disproportionation reaction of VCl 4  with LiSSiPh 3  ; O = V (OSiR 3 ) 3  (R = Me , Ph) undergoes a reaction with Lawesson reagent to yield dithiophosphonate complexes. All compounds obtained are characterized by  1 H and  51 V NMR spectroscopy; the stability of thiovanadium(V) compounds is discussed. V(S t C 4 H 9 ) 4  has been synthesized as a first example of vanadium(IV) thiolates

Oxo-und Thiovanadium(V)-Thiolate/Oxo and Thiovanadium(V) Thiolates