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The titanocene dithiolenato chelates Cp′ 2 Ti(S 2 C 6 H 3 CH 3 -4) and CpCp′Ti(S 2 C 6 H 3 CH 3 -4) (Cp = η 5 -C 5 H 5 , Cp′ = η 5 -C 5 H 4 CH 3 ) were prepared by reaction o f Cp′ 2 TiCl 2  or CpCp′TiCl 2  with equiva­lent amounts of 1,2 -(LiS) 2 C 6 H 3 CH 3 -4. The structure and the conform ational mobility of the η 5 -bonded and of the chelating ligands of the dithiolenato complexes are discussed on the basis of their temperature-dependent  1 H NMR spectra. The mass spectra show metastable transitions for the fragmentation processes.

zeitschrift für naturforschung b

Synthese und Konformationsstudien ringsubstituierter Titanocen-Dithiolen-Chelate / Synthesis and Conform ational Studies of Ring-Substituted Titanocene Dithiolene Chelates