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The iron(II) complexes FeX 2 [P(CH 2 CH 2 CH 2 PMe 2 ) 3 ] with X = CN (4), N 3  (5). and NCS (6) have been prepared by metathetical reaction of FeCl 2 [P(CH 2 CH 2 CH 2 PMe 2 ) 3 ] (1) with the corresponding sodium pseudohalide. Treatment of the dihalo compounds FeX 2 [P(CH 2 CH 2 CH 2 PMe 2 ) 3 ] (X 2  = Cl 2  (1). Br 2  (2), I 2  (3)) with LiAlH 4  gave the halohydro derivatives FeHX[P(CH 2 CH 2 CH 2 PMe 2 ) 3 ], where HX = HCl (7). HBr (8). and HI (9). Consistent with a cis-octahedral coordination geometry, the  31 P NMR spectra of 1−9 exhibit AMX 2  type splitting. The halohydro complexes 7−9 have also been studied by IR and  1 H NMR spectroscopy.  57 Fe Möβbauer data have been collected for compounds 1, 4, and 5.

zeitschrift für naturforschung b

Oligophosphan-Liganden, X II [1] Pseudohalogeno- und Halogenohydridoeisen(II)-Komplexe des tripodal-tetratertiären Phosphanliganden P(CH 2 CH 2 CH 2 PMe 2 ) 3  / Oligophosphine Ligands, X II [1] Pseudohalo and Halohydro Complexes of Iron (II) Containing the Tripod Tetratertiary Phosphine Ligand P(CH 2 CH 2 CH 2 PMe 2 ) 3