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Reaction of HPr i P-CH 2 -PPr i H with Fe 2 (CO) 9  in a molar ratio of 1:2 produces a mixture of cluster compounds from which Fe 4 (CO) 10 [(μ 2 -PPr i ) 2 CH 2 ](μ 2 -PPr i Me)(μ 2 -H)(μ 4 -PH) could be isolated by liquid chromatography. X-ray structural analysis shows a planar trapezoid arrangement for the four iron atoms (Fe1 -Fe2 2,648(1), Fe2 -Fe3 2,790(1), Fe3 -Fe4 2,643(1), Fe1 --Fe4 4,109(1) Å ) capped by the novel bidentate phosphido bridge (μ 2 -PPr i ) 2 CH 2  and the unsubstituted phosphinidene, PH( Fe1 - P4 2,284(1), Fe 2  - P4 2,410(1), Fe3 - P4 2,405(1), Fe4 - P4 2,288(1), P4 - H1 1,39(4) Å).

zeitschrift für naturforschung b

Lineare Oligophosphaalkane, XI [1] Stabilisierung von Phosphiniden, PH, im Clusteryerband — Röntgenstrukturanalyse von Fe 4 (CO) 10 [(μ 2 -PPr i ) 2 CH 2 ](μ 2 -PPr i Me)(μ 2 -H)(μ 4 -PH)