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The reaction of the cubane cluster (C 5 Me 5 ) 2 Cr 2 Co 2 (CO) 2 S 4  with PR 3  (R = Ph, OMe) resulted in a stepwise substitution of CO ligands by PR 3 . One of the reaction products, (C 5 Me 5 ) 2 Cr 2 Co 2 {P(OMe) 3 } 2 S 4 , was characterized by an X-ray diffraction study, confirming that the 60-e core of composition Cr 2 Co 2 S 4  was retained.

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Synthese von PR 3  (R = Ph, OMe) substituierten Cubanclustern vom M 2 M' 2 S 4 -Typ und Molekülstruktur von (C 5 Me 5 ) 2 Cr 2 Co 2 {P(OMe) 3 } 2 (μ 3  -S) 4