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By reaction of COS with malonitrile in presence of potassium ethanolate in ethanol K 2 O(S)CC(CN) 2  · H 2 O is obtained. It reacts with Ba(NCS)2 ·3H 2 O in ethanol to form colourless crystals of BaO(S)CC(CN) 2  · 4H 2 O. The space group of the barium salt is Pn2 1 a (standard: Pna2 1 ) with Z = 4. The structure consists of Ba 2+  and [O(S)CC(CN) 2  ] 2  - ions. The barium ion is bound to three nitrogen and six oxygen atoms. The coordination polyhedron is a tricapped trigonal prism. The anion [O(S)CC(CN) 2  ] 2  - is not exactly planar and is involved in several hydrogen bondings.

zeitschrift für naturforschung b

Zur Darstellung und Kristallstruktur von Barium-1,1-dicyanoethylen-2,2-oxo-thiolat-Tetrahydrat — ein Salz mit dem Anion [O(S)CC(CN) 2  ] 2-  / Synthesis and Crystal Structure of Barium-1,1-dicyanoethylene-2,2-oxo-thiolate Tetrahydrate — a Salt with the Anion [O(S)CC(CN) 2 ] 2-