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The new compound Gd 2 NCl 3  is formed from GdCl 3  with Gd and N 2  as well as from GdCl 3  with GdN (at 1020 K). The crystal structure contains NGd 4  tetrahedra, which are linked via opposite edges to form infinite chains (Orthorhombic, Pbcn; a = 1301.7(1), b = 673.10(6), c = 614.03(7) pm; R = 0.031 for 578 independent reflections). The formal analogy with structures containing condensed clusters, e.g. Gd 2 Cl 3 , is discussed.

Synthese und Kristallstruktur von Gd 2 NCl 3 / Synthesis and Crystal Structure of Gd 2 NCl 3