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[C 4 H 11 N 8 NiO 4 ] + [C 12 H 4 N 4 ] - , M r  = 498.09 is triclinic, P1̄, a = 3.7718(6), b = 7.436(2), c = 17.511(4) Å, α = 88.67(2), β = 86.93(2), γ = 85.05(2)°, V = 488.51 Å 3 , Z = 1, d c  = 1.69 gcm -3 , final R w  = 0.035 for 1454 observed independent reflections. The crystals consist of segregated regular parallel stacks of planar metal complex cations and tenq -  counterions with intermolecular H bonds stabilizing the structure. The compound is metallic at room temperature. A metal to semiconductor transition around 230 K shows up in thermopower data, in the microwave conduc­tivity and epr around 170 K. It is not visible in the static magnetic susceptibility.

zeitschrift für naturforschung b

A Novel Molecular Metal: (Oxamide oximato) (Oxamide oxime)nickel(II). Tetracyanoquinodimethanide, [Ni(oaoH)(oaoH 2 )]tcnq, and Physical Properties of its Semiconducting Pt Analogue