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The photo-induced reaction of CpFe(CO) 2 Et (1) with either trimethylphosphane or trimethylphosphite (L) in solution results in formation of the substitution products CpFe(CO)(L)Et (3), CpFe(L) 2 Et (5), and the hydrido complexes CpFe(CO)(L)H (4), and CpFe(L) 2 H (0). In contrast, the thermal reaction of 1 with L yields the adduct CpFe(CO)(L)COEt (7) and the dimeric compound Cp 2 Fe 2 (CO) 3 L. Under photochemical conditions, the terminal carbonyl ligand in 7 can be replaced by L to give the derivative CpFe(L) 2 COEt (8).

zeitschrift für naturforschung b

Thermische und Photo-induzierte Substitutionsreaktionen an der Eisen-ethyl-Verbindung CpFe(CO) 2 Et. Die Molekülstruktur von CpFe(PMe 3 ) 2 COEt (Cp =η 5 -C 5 H 5 )/ Thermal and Photo-Induced Substitution Reactions of the Iron Ethyl Compound CpFe(CO) 2 Et. The Molecular Structure of CpFe(PMe 3 ) 2 COEt (Cp = η 5 -C 5 H 5 )