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The red, diamagnetic complex [Mo(NO)(terpy)(CN)(HNO)] • 2H 2 O crystallizes in the triclinic space group P1̅(C 1  i -No2) with cell constants a = 867.1(3), b = 1008.4(4), c = 1095.6(3) pm, a = 73.64(3)°, β = 83.54(3)°, γ = 83.16(3)°, and Z = 2. The final R value of the single crystal X-ray analysis is 0.063 for 1922 unique reflections. The structure consists of neutral complexes of [Mo(NO)(terpy)(CN)(HNO)]. The geometry about the molybdenum is a distorted pentagonal bipyramid with a linear NO and CN group in the axial positions, a triclentate terpyridine ligand and an O,N-coordinated HNO 2-  ligand in equatorial positions.

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η 2 -Koordination eines Hydroxylamid(2-)Anions: Die Kristallstruktur von [Mo(NO)(terpy)(CN)(HNO)] 2H 2 O / η 2 -Coordination of a Hydroxylamido(2-) Anion: The Crystal Structure of [Mo(NO)(terpy)(CN)(HNO)]2H 2 O