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The pseudohalogens (XCN) 2  (X = S or Se) react with n-C 5 H 5 Co(CO) 2  and n-Me 3 SiC 5 H 4 Co(CO) 2  with formation of the 18 electron complexes, RCo(CO)(XCN) 2  (R = n-C 5 H 5  or n-Me 3 SiC 5 H 4 ). By reactions with X(CN) 2  (X = S or Se), the cyclopentadienyl cobalt dicarbonyls are transformed into the mixed complexes, RCo(CO)(CN)(XVN) (R = n-C 5 H 5  or n-Me 3 SiC 5 H 4 . All the compounds are characterized by elemental analysis, IR, electronic and  1 H NMR spectra. The thiocyanogen derivatives undergo linkage isomerism (N→S) in polar solvents.

Reactions of n-C 5 H 5 Co(CO) 2 and n-Me 3 SiC 5 H 4 Co(CO) 2 with (XCN) 2 and X(CN) 2 (X = S or Se)