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At room temperature in the presence of CsF sulfur-oxide-chloride-fluoride-imides R f NSOFCl (8) (R f  = CF 3 , C 2 F 5 , i-C 3 F 7 , C 6 F 5 ) are formed from N-perfluoroalkyl-sulfinyl-imides and Cl 2 . At prolonged reaction times or higher temperatures the chloride is ex-changed and the difluorides R f NSOF 2  are isolated in high yields. In the same way (CF 3 ) 2 CFNS(O)ClCF 3  (12) and (CF 3 ) 2 CClNS(O)ClCF 3  (13) are obtained from (CF 3 ) 2 C = N-S(O)CF 3  (9) and Cl 2 /CsF. 12 can be fluorinated by CsF to give (CF 3 )2CFNS(O)FCF 3  (14). 14 is also observed, when fluorine is added to 9 via XeF 2  in the presence of BF 3 , but mainly C-S-bond cleavage occurs. SF 5 NS(O)FCF(CF 3 ) 2  (19) was identified by spectroscopic methods from the reaction of SF 5 NSOF 2  and CF 3 CF = CF 2  in the presence of CsF.

Schwefel(VI)-oxid-chlorid-imide und Schwefel(VI)-oxid-fluorid-imide [1] / Sulfur(VI)-oxide-chloride-imides and Sulfur(VI)-oxide-fluoride-imides [1]