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The spinel system Zn[Fe x V 2-x ]O 4  has been prepared by heating mixtures of ZnV 2 O 4  and ZnFe 2 O 4  at 1000 °C. The lattice constants increase linearly with x by 3.6 pm, the oxygen parameters are constant with a mean value u = 0.384s. The parameters of room temperature Mössbauer spectra show that in the whole series V(III) and Fe(III) are present.

zeitschrift für naturforschung b

Verteilung und Valenz der Kationen in Spinellsystemen mit Eisen und Vanadium, I Röntgenographische und Mößbauer-spektroskopische Untersuchung des Spinellsystems ZnV 2 O 4 -ZnFe 2 O 4  / Distribution and Valence of the Cations in Spinel Systems with Iron and Vanadium, IX-ray Investigation and Mössbauer Spectra of the Spinel System ZnV 2 O 4 -ZnFe 2 O 4