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Bromo-Elpasolites of formulae Cs 2 LiMBr 6  and Cs 2 NaMBr 6  (M = Sc, Y, La-Lu, In, V, Cr) were prepared and investigated by powder X-ray diffraction. The compounds Cs 2 NaMBr 6  (M = Ce-Lu, Sc, Y, In) as well as Cs 2 LiMBr 6  (M = La-Er, Y) crystallize cubic facecentered (elpasolite type of structure); Cs 2 NaLaBr 6  and low temperature forms of Cs 2 NaMBr 6  (M = Ce-Gd) are tetragonal. Several hexagonal crystal structure types (HT-K 2 LiAlF6, Cs 2 NaCrF 6 , Cs 2 LiGaF 6 ) are observed for Cs 2 LiMBr 6  (M = Tm, Yb, Lu, Sc, In, V, Cr).

zeitschrift für naturforschung b

Halogen-Elpasolithe, IV [1]. Über Brom-Elpasolithe Cs 2 B I M III Br 6  B I  = Li, Na; M III  = Sc, Y, La-Lu, In, V, Cr) / Halo-Elpasolites, IV [1]. On Bromo-Elpasolites  Cs 2 B I M III Br 6  B I  = Li, Na; M III  = Sc, Y, La-Lu, In, V, Cr)