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Lithium-2-methylmercaptobenzol-1-thiolat reacts with C 5 H 5 Fe(CO) 2 Cl to give [C 5 H 5 Fe(CO) 2 (S-C 6 H 4 -SCH 3 ]); with C 5 H 5 Mo(CO) 3 Cl cleavage of metal chlorine and metal carbonyl bonds occurs yielding [C 5 H 5 Mo(CO) 2 (S-C 6 H 4 -SCH 3 )]. Reaction of dilithium- benzene-1,2-dithiolate with C 5 H 5 Fe(CO) 2 Cl leads to the binuclear [{C 5 H 5 Fe(CO) 2 } 2 S 2 C 6 H 4 ]. CO substitution and rearrangement are observed on irradiation of the complexes yielding [μ-S 2 C 6 H 4 {C 5 H 5 Fe(CO)} 2 ], [C 5 H 5 Fe(CO)(S-C 6 H 4 -SCH 3 )] and [C 5 H 5 Fe(μ-S 2 C 6 H 4 )] 2 . Syn­theses, properties and spectra of the complexes are reported and discussed.

zeitschrift für naturforschung b

Synthese und Eigenschaften von Eisen-und Molybdän-Komplexen mit Schwefelliganden [1] / Synthesis and Properties of Iron and Molybdenum Complexes with Sulfur Ligands [1]