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Bis(trimethylsilyl)diazene reacts with cyclopentadienyl metal chlorides with reduction followed by addition. According to X-ray analysis the chromium complex [C 5 H 5 Cr(NSiMe 3 ) 2 ] 2 , formed by the reaction of C 5 H 5 CrCl 2  with azosilane, contains tri-methylsilylazene ligands. The addition of Me 3 Si-N = N-SiMe 3  to chromium is therefore connected with a cleavage of the azo group in this case.

zeitschrift für naturforschung b

Darstellung und Struktur des Komplexes [C 5 H 5 Cr(NSiMe 3 ) 2 ] 2  (Zur Reaktion von Cyclopentadienylmetallchloriden mit Bis(trimethylsilyl)diazen)/Preparation and Structure of the Complex [C 5 H 5 Cr(NSiMe 3 ) 2 ] 2  (Reaction of Cyclopentadienylmetal Chlorides with Bis(trimethylsilyl)diazene)