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The new compound BaSb 3  has been prepared and its structure determined. It crystallizes monoclinic (C 2/m, a = 1080.7(5) pm, b = 851.9(5) pm, c = 647.1(5) pm, β = 112.66(4)°). The Sb-atoms build up 14-rings of two-and threebonded Sb, which are connected to puckered nets.

zeitschrift für naturforschung b

BaSb 3 , ein Antimonid mit einem zweidimensional unendlichen [Sb 3  2- ] n -Polyanion / BaSb 3 , an Antimonide with an Infinite Twodimensional [Sb 3  2- ] n  - Anion