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The new ternary tin(II) sulfide iodide Sn 4 SI 6  was prepared by annealing of stoichiometric amounts of SnI 2  and SnS at 280 °C. The structure of this compound was determined from three-dimensional X-ray data. The cell parameters for the monoclinic phase are a = 14.129, b = 4.425, c = 25.15 Å, and β = 93.42°; space group C2/m (No. 12), Z = 4. Parts of the structure are built up of the Snl 2  structure.

Die Kristallstruktur des Zinnsulfidiodids Sn 4 SI 6 / The Crystal Structure of Sn 4 SI 6