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The preparation of the 1:1:1 addition compound 1 of 1,4-dioxane, water and antimony(V) chloride is described. 1 crystallizes in the space group Cmcm with the lattice constants a = 8.494, b = 11.453, c = 13.030 Å with four formula units in the unit cell. The dioxane is strongly hydrogen bonded to an antimony(V) chloride water adduct. The vibrational spectra of the solid are assigned

zeitschrift für naturforschung b

1.4-Dioxan · H 2 O · SbCl 5 ; Schwingungsspektren, Kristall- und Molekülstruktur / 1,4-Dioxane · H 2 O · SbCl 5 ; Vibrational Spectra, Crystal and Molecular Structure