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The monomelic and readily soluble compounds R 2 PO 2 Re(CO) 3 diphos (1a, b) [R = CH 3 : (a); C 6 H 5 : (b)], in which diphos and R 2 PO 2 - are linking bidentate i.e. unidentate to rhenium, are obtained by reaction of [R 2 PO 2 Re(CO) 3 THF] n  with diphos. Heating 1 a to 110 °C the polymeric complex [(CH 3 ) 2 PO 2 Re(CO) 2 diphos] n  (2) is formed. The IR, Raman, and  31 P NMR spectra are discussed.

zeitschrift für naturforschung b

Das Verhalten von Phosphinato-Komplexen des Rheniums gegenüber 1.2-Bis(diphenylphosphin)ethan / The Behaviour of Phosphinato Complexes of Rhenium towards 1,2-Bis(diphenylphosphine)ethane