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Results from temperature-jump relaxation measurements indicate the existence of an intermediate, the pentaoxoiodate(VII)monoanion, in the hydration-dehydration equilibrium between hexa- and tetraoxoiodate(VII)monoanions in aqueous solution. The interconversion is accompanied by a considerable reorientation of the water molecules solvating the monoanionic species, which play a crucial rôle in the mechanism of hydration and dehyd ation. This is the first definite evidence for the existence of a penta coordinated periodate species in aqueous solution.

Notizen: Pentaoxoiodate(VII)monoanion as an Intermediate in the Interconversion of Hexa- and Tetraoxoiodate(VII)monoanions in Aqueous Solution