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The crystal structure of (PyH) 2 (Mo 2 O 4 Cl 4 ) · 3 H 2 O, earlier formulated as tetrameric di-μ-oxo-bis(di-µ-oxo-oxotetrachloroaquodimolybdate(V)), [(PyH) 4 ][Mo 4 O 8 Cl 8 (H 2 O) 2 ], has been determined. The structure consists of the dimeric anions [Mo 2 O 4 Cl 4 ] 2 - with strong Mo=O ••• Mo interactions along the short c axes (c = 4.11 Å). The polymeric

zeitschrift für naturforschung b

Darstellung, Infrarotspektren und Strukturen einiger dimerer und polymerer Oxochloro- und Oxooxalato-isothiocyanato-Komplexe des Molybdän(V).: Synthesis, Infrared Spectra and Structure of Some Dimeric and Polymeric Oxochloro and Oxooxalato-isothiocyanato Complexes of Molybdenum(V)