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The rotational spectra of m-xylene, (CH 3 ) 2 C 6 H 4  and of m-xylene-d 10 , (CD 3 ) 2 C 6 D 4  have been recorded between 6 and 26.5 GHz using pulsed beam Fourier transform microwave spectroscopy. The clue for the assignment of the internal rotation multiplets was the inertial defect derived from the A 1 A 1  species transitions.

The Microwave Spectra of m-Xylene and m-Xylene-d 10 . Determination of the Low Methyl Internal Rotation Barrier