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The crystal structure of the high temperature phase of anilinium bromide, C 6 H 5 NH 3  ⊕ Br ⊖  , was studied by X-ray and neutron diffraction at T = 343 K. The refinement supports disordered positions of the -NH 3  ⊕  group. A split-atom model is proposed which includes disorder of the benzene ring. The thermal parameters, hydrogen bond distances, and other experimental data (NMR, NQR, inelastic neutron scattering) are in accordance with this model.

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On the Order-Disorder Phase Transformation of Anilinium Halides. III.: III. High Temperature Phase Crystal Structure of Anilinium Bromide, C 6 H 5 NH 3  ⊕ Br ⊖ . An X-ray and Neutron Diffraction Study