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C 15 H 13 BF 9 N 7 NiO, orthorhombic,  Pnma  (no. 62),  a  = 17.8513(3) Å,  b  = 13.3869(2) Å,  c  = 8.5944(2) Å,  V  = 2053.83(7) Å 3 ,  Z  = 4,  R gt   ( F ) = 0.0235,  wR ref   ( F   2 ) = 0.0690,  T  = 124(2) K.

The crystal structure of nitroxyl- κ N -{hydridotris(3-trifluoromethyl-5-methylpyrazolyl-1-yl- κN 3 )borato}nickel(II), C 15 H 13 BF 9 N 7 NiO