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C 27 H 49 ClN 4 NiO 12 , triclinic,  P1   ‾$\overline{1}$(no. 2),  a  = 11.180(2) Å,  b  = 12.320(3) Å,  c  = 12.754(3) Å,  α  = 98.263(2)°,  β  = 97.524(2)°,  γ  = 99.470(2)°,  V  = 1693.1(6) Å 3 ,  Z  = 2,  R  gt ( F ) = 0.0423, w R  ref ( F  2 ) = 0.1238,  T  = 296(2) K.

zeitschrift für kristallographie - new crystal structures

Crystal structure of  catena -poly[(5,5,7,12,12,14-hexamethyl -1,4,8,11-tetraazacyclotetradecane-  κ  4  N , N ′, N ʺ, N‴ )nickel(II)-(μ 2 -perchlorato- κ  2  O : O ′)] 3,5-dicarboxybenzoate – methanol (1/2), C 27 H 49 ClN 4 NiO 12