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C 8 H 6 ClN, orthorhombic,  Pnma  (no. 62),  a  = 20.3965(7) Å,  b  = 7.8164(3) Å,  c  = 4.5015(2) Å,  V  = 717.66(5) Å 3 ,  Z  = 4,  R    gt   ( F ) = 0.0265,  wR    ref   ( F  2 ) = 0.0670, T = 100.0 K.

The crystal structure of 4-(chloromethyl)benzonitrile, C 8 H 6 ClN