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C 20 H 22 F 6 I 2 N 3 Sb, triclinic,P1   ‾$P\bar{1}$(no. 2),  a  = 10.2268(10) Å,  b  = 10.8850(9) Å,  c  = 12.1413(10) Å,  α  =  101.810(2)°,  β  = 90.465(3)°,  γ  = 103.194(3)°,  V  = 1285.9(2) Å 3 ,  Z  = 2,  Rgt   ( F ) = 0.0291,  wRref   ( F   2 ) = 0.0717, T = 200 K.

The crystal structure of 4,5-diiodo-1,3-dimesityl-1 H -1,2,3-triazol-3-ium hexafluoridoantimonate(V), C 20 H 22 F 6 I 2 N 3 Sb