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Zn   2    C  8    H   32N  4    O   16S  4${\text{Zn}}_{2}{\text{C}}_{8}{\text{H}}_{32}{\text{N}}_{4}{\text{O}}_{16}{\text{S}}_{4}$, triclinic,P    1  ‾$P&amp;#x203e;{1}$(no. 2),  a  = 9.0313(9) Å,  b  = 9.6075(14) Å,  c  = 15.3044(15) Å,  α  = 89.933(2)°,  β  = 78.579(1)°,  γ  = 68.878(1)°,  V  = 1210.6(2) Å 3 ,  Z  = 2,R   g  t${R}_{gt}$( F ) = 0.0323,w   R   ref$w{R}_{\mathit{ref}}$( F  2 ) = 0.1043,  T  = 100(2) K.

A new polymorph of tetrakis(dimethylammonium) catena -poly[tetrakis( μ 2 -sulfato- κ 2 O:O ′)dizinc(II)], Zn 2 C 8 H 32 N 4 O 16 S 4