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C 23 H 44 ClN 5 NiO 7 , orthorhombic,  P 2 1 2 1 2 1  (no. 19),  a  = 14.4994(16) Å,  b  = 19.799(2) Å,  c  = 20.040(2) Å,  V  = 5752.9(11) Å 3 ,  Z  = 8,  R  gt ( F ) = 0.0409,  wR  ref ( F  2 ) = 0.1061,  T  = 173(2) K.

zeitschrift für kristallographie - new crystal structures

Crystal structure of (4-aminobenzoato-κ 2  O , O′ )-[5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ 4  N , N′ , N′′ , N′′′ ]nickel(II) perchlorate monohydrate, C 23 H 44 ClN 5 NiO 7