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C 24 H 18 O 2 , orthorhombic,  Ccc 2 (no. 37),  a  = 9.7401(14) Å,  b  = 34.509(5) Å,  c  = 21.970(3) Å,  V  = 7384.7(19) Å 3 ,  Z  = 16,  R  gt ( F ) = 0.0738,  wR  ref ( F  2 ) = 0.1559,  T  = 298(2) K.

The crystal structure of 1,2-bis((4-methoxyphenyl)ethynyl)benzene, C 24 H 18 O 2