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C 29 H 50 Cl 2 N 4 NiO 8 , orthorhombic,  Pbca  (no. 61),  a  = 20.601(3) Å,  b  = 13.5059(16) Å,  c  = 25.015(3) Å,  Z  = 8,  V  = 6960.3(15) Å 3 ,  R  gt ( F ) = 0.0495,  wR  ref ( F  2 ) = 0.1652,  T  = 296(2) K.

zeitschrift für kristallographie - new crystal structures

Crystal structure of [(2-(2-chlorophenyl)-5-ethyl-1,3-dioxane-5-carboxylato-κ 2  O , O′ ) (5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ 4  N , N′ , N′′ , N′′′ )]nickel(II) perchlorate, C 29 H 50 Cl 2 N 4 NiO 8