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The title compound Bu 2 NH 2 (PhPO 3 H) 2 SnMe 3  was synthesized and its structure determined by single crystal X-ray crystallography. The structure consists of two monodentate hydrogenophosphonates [PhPO 3 H] -  bonded to SnMe 3  groups leading to SnC 3 O 2  moiety in a  trans  trigonal bipyramidal environment. [(PhPO 3 H) 2 SnMe 3 ] -  dimerizes through hydrogen bonds. Dibutylammonium (Bu 2 NH 2  + ) cations are hydrogen bonded to the dimeric moieties through phosphonates to give a chain structure.

Supramolecular architecture in crystalline Bu 2 NH 2 (PhPO 3 H) 2 SnMe 3