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A series of nitrogen-doped TiO 2  nanostructured photocatalysts were synthesized by oxidizing titanium nitride at different temperatures under ambient condition. The as-prepared samples were systematically characterized by X-ray diffraction, transmission electron microscopy, X-ray photoelectron spectroscopy (XPS), and ultraviolet-visible (UV-Vis) absorption spectra. The photocatalytic activity for hydrogen evolution of the as-prepared samples was evaluated under UV-Vis light irradiation. XPS investigations confirmed the presence of nitrogen in TiO 2  lattice in the chemical environment of O−Ti−N. The UV-Vis absorption spectra results showed that the absorption edge was extended into visible light region. Higher photocatalytic activity than that of commercial titanium dioxide - P25 was observed over the as-prepared nitrogen-doped TiO 2  under UV-Vis light illumination.

Nitrogen-doped TiO 2 Photocatalysts Synthesized from Titanium Nitride: Characterizations and Photocatalytic Hydrogen Evolution Performance